Technology Process of 2,2',3'-tri-O-acetyl-p-scrobiculin
There total 7 articles about 2,2',3'-tri-O-acetyl-p-scrobiculin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 89 percent / K2CO3 / acetone / 18 h / Heating
2: 92 percent / aq. KOH / dimethylsulfoxide / 20 h / 70 °C
3: 75 percent / trifluoroacetic anhydride / benzene / 6 h / Ambient temperature
4: 82 percent / H2 / 10percent Pd/C / ethyl acetate
5: 97 percent / pyridine / 3 h / Ambient temperature
With
pyridine; potassium hydroxide; hydrogen; potassium carbonate; trifluoroacetic anhydride;
palladium on activated charcoal;
In
dimethyl sulfoxide; ethyl acetate; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / pyridine / 2 h / Ambient temperature
2: 92 percent / H2 / 10percent Pd/C / ethyl acetate / 2.5 h
3: 75 percent / trifluoroacetic anhydride / benzene / 6 h / Ambient temperature
4: 82 percent / H2 / 10percent Pd/C / ethyl acetate
5: 97 percent / pyridine / 3 h / Ambient temperature
With
pyridine; hydrogen; trifluoroacetic anhydride;
palladium on activated charcoal;
In
ethyl acetate; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 75 percent / trifluoroacetic anhydride / benzene / 6 h / Ambient temperature
2: 82 percent / H2 / 10percent Pd/C / ethyl acetate
3: 97 percent / pyridine / 3 h / Ambient temperature
With
pyridine; hydrogen; trifluoroacetic anhydride;
palladium on activated charcoal;
In
ethyl acetate; benzene;
