C₁₆H₂₂O₃

Base Information

Chemical Name:C₁₆H₂₂O₃
CAS No.:1609268-85-0
Molecular Formula:C₁₆H₂₂O₃
Molecular Weight:262.349
Hs Code.:

C<sub>16</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₁₆H₂₂O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₂₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₂₂O₃

There total 10 articles about C₁₆H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609268-88-3
C₂₈H₃₇NO₆

: 1609268-85-0
C₁₆H₂₂O₃

Guidance literature:: With hydrogenchloride; lithium hydroxide hydrate; In tetrahydrofuran; water; at 0 - 80 ℃; for 16.5h; Inert atmosphere;
DOI:10.3987/COM-13-12905

Reference yield:

: C₁₇H₂₆O₅

: 1609268-85-0
C₁₆H₂₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; pivaloyl chloride / tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

1.2: 4 h / -20 - 20 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 3.5 h / Inert atmosphere

3.1: lithium hydroxide hydrate; hydrogenchloride / water; tetrahydrofuran / 16.5 h / 0 - 80 °C / Inert atmosphere

With hydrogenchloride; lithium hydroxide hydrate; sodium hexamethyldisilazane; pivaloyl chloride; triethylamine; In tetrahydrofuran; water;
DOI:10.3987/COM-13-12905

Reference yield:

: C₁₅H₂₂O₄

: 1609268-85-0
C₁₆H₂₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzene / 6.5 h / 80 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: lithium hydroxide hydrate / water; tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

4.1: triethylamine; pivaloyl chloride / tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

4.2: 4 h / -20 - 20 °C / Inert atmosphere

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

5.2: 3.5 h / Inert atmosphere

6.1: lithium hydroxide hydrate; hydrogenchloride / water; tetrahydrofuran / 16.5 h / 0 - 80 °C / Inert atmosphere

With hydrogenchloride; lithium hydroxide hydrate; palladium 10% on activated carbon; hydrogen; sodium hexamethyldisilazane; pivaloyl chloride; triethylamine; In tetrahydrofuran; water; benzene; 1.1: |Wittig Olefination;
DOI:10.3987/COM-13-12905