Technology Process of C37H52N6O10
There total 9 articles about C37H52N6O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere
2: triethylamine; dmap / acetonitrile / Inert atmosphere
3: 2,2'-azobis(isobutyronitrile) / Reflux; Inert atmosphere
With
dmap; 2,2'-azobis(isobutyronitrile); triethylamine tris(hydrogen fluoride); triethylamine;
In
acetonitrile;
DOI:10.1021/jo500039d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
2: toluene / 48 h / 70 °C / Inert atmosphere
3: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere
4: triethylamine; dmap / acetonitrile / Inert atmosphere
5: 2,2'-azobis(isobutyronitrile) / Reflux; Inert atmosphere
With
dmap; 2,2'-azobis(isobutyronitrile); sodium hydrogencarbonate; triethylamine tris(hydrogen fluoride); triethylamine;
In
N,N-dimethyl-formamide; toluene; acetonitrile;
2: |Ugi Condensation;
DOI:10.1021/jo500039d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene / 48 h / 70 °C / Inert atmosphere
2: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere
3: triethylamine; dmap / acetonitrile / Inert atmosphere
4: 2,2'-azobis(isobutyronitrile) / Reflux; Inert atmosphere
With
dmap; 2,2'-azobis(isobutyronitrile); triethylamine tris(hydrogen fluoride); triethylamine;
In
toluene; acetonitrile;
1: |Ugi Condensation;
DOI:10.1021/jo500039d
