C₂₄H₃₇BO₅Si

Base Information

Chemical Name:C₂₄H₃₇BO₅Si
CAS No.:1519887-93-4
Molecular Formula:C₂₄H₃₇BO₅Si
Molecular Weight:444.451
Hs Code.:

C<sub>24</sub>H<sub>37</sub>BO<sub>5</sub>Si

Synonyms:

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Chemical Property of C₂₄H₃₇BO₅Si

Chemical Property:

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Technology Process of C₂₄H₃₇BO₅Si

There total 9 articles about C₂₄H₃₇BO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₄₀O₄Si

: 1519887-93-4
C₂₄H₃₇BO₅Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 °C

2.1: ammonium fluoride / ethanol; methanol / 24 h

3.1: triphenylphosphine / tetrachloromethane / 12 h / Reflux

4.1: sodium; Iron(III) nitrate nonahydrate; ammonia / 2 h / -40 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 14 h / 0 - 20 °C

6.1: C₇H₁₂BI / pentane / 1 h / 0 - 20 °C / Darkness

6.2: 0.17 h / 0 °C

7.1: silver nitrate; triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

8.1: hydrogen / methanol / 6 h / 760.05 Torr

9.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / dichloromethane; tetrahydrofuran / 72 h

With 2,6-dimethylpyridine; Iron(III) nitrate nonahydrate; ammonium fluoride; osmium(VIII) oxide; C₇H₁₂BI; 1,3-bis-(diphenylphosphino)propane; ammonia; hydrogen; palladium diacetate; sodium; potassium carbonate; silver nitrate; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; pentane;
DOI:10.1021/jo402537u

Reference yield:

: 1519887-74-1
methyl [2R,2(1S),3R,5S]-5-(hydroxymethyl)-3-methyl-2-(1-methylcyclohex-2-en-1-yl)tetrahydrofuran-2-carboxylate

: 1519887-93-4
C₂₄H₃₇BO₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: triphenylphosphine / tetrachloromethane / 12 h / Reflux

2.1: sodium; Iron(III) nitrate nonahydrate; ammonia / 2 h / -40 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 14 h / 0 - 20 °C

4.1: C₇H₁₂BI / pentane / 1 h / 0 - 20 °C / Darkness

4.2: 0.17 h / 0 °C

5.1: silver nitrate; triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

6.1: hydrogen / methanol / 6 h / 760.05 Torr

7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / dichloromethane; tetrahydrofuran / 72 h

With 2,6-dimethylpyridine; Iron(III) nitrate nonahydrate; osmium(VIII) oxide; C₇H₁₂BI; 1,3-bis-(diphenylphosphino)propane; ammonia; hydrogen; palladium diacetate; sodium; silver nitrate; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; dimethyl sulfoxide; pentane;
DOI:10.1021/jo402537u

Reference yield:

: 1519887-83-2
methyl [2R,2(1S),3R]-2-hydroxy-2-(1-methylcyclohex-2-en-1-yl)-3-methylhex-5-ynoate

: 1519887-93-4
C₂₄H₃₇BO₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 14 h / 0 - 20 °C

2.1: C₇H₁₂BI / pentane / 1 h / 0 - 20 °C / Darkness

2.2: 0.17 h / 0 °C

3.1: silver nitrate; triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

4.1: hydrogen / methanol / 6 h / 760.05 Torr

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / dichloromethane; tetrahydrofuran / 72 h

With 2,6-dimethylpyridine; osmium(VIII) oxide; C₇H₁₂BI; 1,3-bis-(diphenylphosphino)propane; hydrogen; palladium diacetate; silver nitrate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; pentane;
DOI:10.1021/jo402537u