-Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate

Base Information

Chemical Name:-Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate
CAS No.:155768-60-8
Molecular Formula:C₂₆H₃₁NO₆
Molecular Weight:453.535
Hs Code.:

<S-(Z)>-Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate

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Technology Process of -Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate

There total 6 articles about -Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21461-84-7
(2S)-tetrahydro-5-oxofuran-2-carboxylic acid

: 155768-60-8
-Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / Heating

2: TEA / CH₂Cl₂ / 0 °C

3: 75 percent / NaOEt / CH₂Cl₂ / 0.5 h / Ambient temperature

4: triethylamine / CH₂Cl₂ / 48 h / Ambient temperature

With thionyl chloride; TEA; sodium ethanolate; triethylamine; In dichloromethane;
DOI:10.1021/jo00087a026

Reference yield:

: 54848-33-8
(S)-tetrahydro-5-oxo-2-furancarbonyl chloride

: 155768-60-8
-Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: TEA / CH₂Cl₂ / 0 °C

2: 75 percent / NaOEt / CH₂Cl₂ / 0.5 h / Ambient temperature

3: triethylamine / CH₂Cl₂ / 48 h / Ambient temperature

With TEA; sodium ethanolate; triethylamine; In dichloromethane;
DOI:10.1021/jo00087a026

Reference yield:

: 155768-36-8
(Z)-5-(4-Methoxyphenyl)-4-penten-1-amine

: 155768-60-8
-Ethyl 4-(benzoyloxy)-5-<<5-(4-methoxyphenyl)-4-pentenyl>amino>-5-oxopentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: TEA / CH₂Cl₂ / 0 °C

2: 75 percent / NaOEt / CH₂Cl₂ / 0.5 h / Ambient temperature

3: triethylamine / CH₂Cl₂ / 48 h / Ambient temperature

With TEA; sodium ethanolate; triethylamine; In dichloromethane;
DOI:10.1021/jo00087a026