Re(CC-4-ethynyl-C₆H₄)(CO)3(N,N'-dimethylpiperazine)

Base Information

Chemical Name:Re(CC-4-ethynyl-C₆H₄)(CO)3(N,N'-dimethylpiperazine)
CAS No.:1147421-54-2
Molecular Formula:C₁₉H₁₉N₂O₃Re
Molecular Weight:509.578
Hs Code.:

Re(CC-4-ethynyl-C<sub>6</sub>H<sub>4</sub>)(CO)3(N,N'-dimethylpiperazine)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Re(CC-4-ethynyl-C₆H₄)(CO)3(N,N'-dimethylpiperazine)

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Technology Process of Re(CC-4-ethynyl-C₆H₄)(CO)3(N,N'-dimethylpiperazine)

There total 1 articles about Re(CC-4-ethynyl-C₆H₄)(CO)3(N,N'-dimethylpiperazine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 106-58-1
N,N'-dimethylpiperazine

: 1147421-44-0
(4-(triisopropylethynyl)phenylacetylide)(tricarbonyl)(N,N'-dimethylpiperazine)rhenium(I)

: 7732-18-5
water

: 1147421-54-2
Re(CC-4-ethynyl-C₆H₄)(CO)3(N,N'-dimethylpiperazine)

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; (N2) a soln. of tetrabutylammonium fluoride in non-dried THF was added to a soln. of complex and diamine in THF, the mixt. was stirred for 20 min, diluted with CH2Cl2 and water; washed with satd. soln. of NaHCO3, an aq. layer was extd. with CH2Cl2, the organic soln. was dried over MgSO4, the solvent was removed in vac., column chromy., toluene-ethyl acetate 4:1 v/v; elem. anal.;
DOI:10.1016/j.ica.2008.07.031