tetrakis(2,6-difluorophenylporphinato)chloroiron(III)

Base Information

Chemical Name:tetrakis(2,6-difluorophenylporphinato)chloroiron(III)
CAS No.:379217-61-5
Molecular Formula:C₄₄H₂₀ClF₈FeN₄
Molecular Weight:855.893
Hs Code.:

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Chemical Property of tetrakis(2,6-difluorophenylporphinato)chloroiron(III)

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Technology Process of tetrakis(2,6-difluorophenylporphinato)chloroiron(III)

There total 1 articles about tetrakis(2,6-difluorophenylporphinato)chloroiron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: H₂N₄(C₄⁽²⁾H₂)4(CC₆H₃F₂)4

: iron(II) chloride

: 379217-61-5
tetrakis(2,6-difluorophenylporphinato)chloroiron(III)

Guidance literature:: With HCl; In N,N-dimethyl-formamide; to refluxing soln. F8TPPH2-d8 in DMF under Ar was added excess FeCl2 andrefluxed for 1 h, react. mixt. was cooled and exposed to air, aq. HCl w as added; ppt. was filtered, dissolved in CH2Cl2 and passed through silica column,solvent was removed, pptn. from CH2Cl2 with heptane;
DOI:10.1021/ic0105866

Reference yield:

: 379217-61-5
tetrakis(2,6-difluorophenylporphinato)chloroiron(III)

: 379217-63-7
iron(II) tetrakis(2,6-difluorophenyl)porphyrinate-d8

Guidance literature:: With sodium hydrosulfite; In dichloromethane; water; under Ar to soln. (F8TPP-d8)Fe(III)Cl in CH2Cl2 was added aq. sodium hydrosulfite and agitaged with Ar bubbling for 30 min; organic layer was concd. and heptane was added;
DOI:10.1021/ic0105866