OsI{PCH₃CO(CF₃)}(CO)2(P(C₆H₅)3)2

Base Information

Chemical Name:OsI{PCH₃CO(CF₃)}(CO)2(P(C₆H₅)3)2
CAS No.:103932-30-5
Molecular Formula:C₄₁H₃₃F₃IO₃OsP₃
Molecular Weight:1040.73
Hs Code.:

OsI{PCH<sub>3</sub>CO(CF<sub>3</sub>)}(CO)2(P(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of OsI{PCH₃CO(CF₃)}(CO)2(P(C₆H₅)3)2

Chemical Property:

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Technology Process of OsI{PCH₃CO(CF₃)}(CO)2(P(C₆H₅)3)2

There total 7 articles about OsI{PCH₃CO(CF₃)}(CO)2(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 103932-33-8
Os{PCO(CF₃)}(CO)2(P(C₆H₅)3)2

: 103932-30-5
OsI{PCH₃CO(CF₃)}(CO)2(P(C₆H₅)3)2

Guidance literature:: With methyl iodide; In dichloromethane; byproducts: hydrogen chloride; heated at reflux for 1 h; cooled; addn. of ethanol;; concentration in vacuo; elem. anal.;
DOI:10.1016/0022-328X(88)80325-5

Reference yield:

: 103932-34-9
[OsCl(PHCOCF₃)(CO)2(P(C₆H₅)3)2]

: 103932-31-6
[OsCl(P(CH₃)COCF₃)(CO)2(P(C₆H₅)3)2]

: 103932-30-5
[OsI(P(CH₃)COCF₃)(CO)2(P(C₆H₅)3)2]

Guidance literature:: With CH₃I; 1,8-diazabicyclo[5.4.0]undec-7-ene; In not given; elem. anal.;
DOI:10.1039/c39850001594

Reference yield:

: 103932-37-2,116948-50-6
{OsCl(PH₃)(CO)2(PPh₃)2}ClO₄

: 103932-31-6
[OsCl(P(CH₃)COCF₃)(CO)2(P(C₆H₅)3)2]

: 103932-30-5
[OsI(P(CH₃)COCF₃)(CO)2(P(C₆H₅)3)2]

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / not given

2: not given

3: CH₃I; 1,8-diazabicyclo[5.4.0]undec-7-ene / not given

With 1,8-diazabicyclo[5.4.0]undec-7-ene; CH₃I; In not given;
DOI:10.1039/c39850001594