(diphenylgermyl)dilithium

Base Information

Chemical Name:(diphenylgermyl)dilithium
CAS No.:120154-49-6
Molecular Formula:C₁₂H₁₀GeLi₂
Molecular Weight:240.683
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (diphenylgermyl)dilithium

Chemical Property:

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Technology Process of (diphenylgermyl)dilithium

There total 1 articles about (diphenylgermyl)dilithium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1675-58-7
diphenylgermane

: 120154-49-6
(diphenylgermyl)dilithium

Guidance literature:: With lithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; under Ar, small pieces of Li stirred vigorously in anhyd. HMPA and THF,Ph2GeH2 in THF added dropwise, reacted for about 40 min; not isolated; determined by hydrolysis with D2O;
DOI:10.1246/bcsj.58.1443

Reference yield: 33.0%

: 120154-49-6
(diphenylgermyl)dilithium

: 938-18-1
mesitylene-2-carboxylic acid chloride

: 124242-66-6
(C₆H₅)2Ge(COC₆H₂(CH₃)3)2

: 1675-58-7
diphenylgermane

: 7366-23-6
diphenylchlorogermane

Guidance literature:: In tetrahydrofuran; ethanol; inert atmosphere; -40°C (15 min), then stirring (20°C, 3 h); hydrolysis (aq. NaHCO3), extn., drying, concentration (vac.), distn. (vac.); elem. anal.;
DOI:10.1021/om00115a032