bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum⁽⁰⁾

Base Information

Chemical Name:bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum⁽⁰⁾
CAS No.:125669-14-9
Molecular Formula:C₃₄H₃₈O₂P₂Pt
Molecular Weight:735.702
Hs Code.:

bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum<sup>(0)</sup>

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Chemical Property of bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum⁽⁰⁾

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Technology Process of bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum⁽⁰⁾

There total 3 articles about bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 12130-66-4
bis(cycloocta-1,5-diene)platinum⁽⁰⁾

: 91533-65-2
diphenyl(tetrahydro-2-furanylmethyl)phosphane

: 125669-14-9
bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum⁽⁰⁾

Guidance literature:: In hexane; without air, moisture; (Ar or N2); addn. of Ph2P(CH2)3CHCH2O in n-hexane to suspension of Pt(COD)2 in n-hexane within 1 h; pptn. of yellow solid; evapn. to ca. 1/3 of volume; separation at -30°C; filtn.; washing with a small amount of cold n-hexane; drying in high-vac.; elem. anal.;

Reference yield: 62.0%

: 16940-66-2
sodium tetrahydroborate

: 124751-48-0,124634-83-9
cis-((C₆H₅)2PCH₂C₄H₇O)2Cl₂platinum(II)

: 125669-14-9
bis(diphenyltetrahydrofuranylmethylphosphan-O,P)platinum⁽⁰⁾

Guidance literature:: In ethanol; exclusion of air, moisture; (Ar or N2); addn. of Ph2P(CH2)3CHCH2O in ethanol to NaBH4 within 0.5 h; stirred for 2 h at 25°C; brown soln.; addn. of H2O; pptd. yellow solid; filtn.; washing with ethanol/water; drying in high-vac.; elem. anal.;