1,1'-trimethylenedicyclopentadienyl(tolyl)lanthanum tetrahydrofuran complex

Base Information

Chemical Name:1,1'-trimethylenedicyclopentadienyl(tolyl)lanthanum tetrahydrofuran complex
CAS No.:105180-41-4
Molecular Formula:C₂₄H₂₉LaO
Molecular Weight:472.399
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Chemical Property of 1,1'-trimethylenedicyclopentadienyl(tolyl)lanthanum tetrahydrofuran complex

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Technology Process of 1,1'-trimethylenedicyclopentadienyl(tolyl)lanthanum tetrahydrofuran complex

There total 1 articles about 1,1'-trimethylenedicyclopentadienyl(tolyl)lanthanum tetrahydrofuran complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 75857-12-4
1,1'-trimethylenedicyclopentadienyllanthanum chloride

: 2417-95-0
p-tolyllithium

: 105180-41-4
1,1'-trimethylenedicyclopentadienyl(tolyl)lanthanum tetrahydrofuran complex

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; byproducts: LiCl; warming a solution of equivalent amounts of 1,1'-trimethylenedicyclopentadienyllanthanum chloride and tolyllithium under Ar from -70 to 25°C (2 hours), stirring for 18 hours and evaporation;; repeated extraction with benzene, evaporation, washing with hexane and drying; elem. anal., (1)H-NMR- and IR spectroscopy;;
DOI:10.1016/0022-328X(86)80080-8