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Technology Process of 9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine

9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine

Base Information
  • Chemical Name:9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine
  • CAS No.:274905-51-0
  • Molecular Formula:C31H30N5O7P
  • Molecular Weight:615.582
  • Hs Code.:
9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ<sup>5</sup>-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine

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Chemical Property of 9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine
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Technology Process of 9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine

There total 1 articles about 9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5'-O-dimethoxytrityladenosine
57018-82-3,81352-25-2

5'-O-dimethoxytrityladenosine

9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ<sup>5</sup>-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine
274905-51-0

9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine

Guidance literature:
With diphenyl hydrogen phosphite; In pyridine; for 0.333333h;
DOI:10.1016/S0040-4039(00)00132-5

Reference yield:

9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ<sup>5</sup>-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine
274905-51-0

9-{(3aR,4R,6R,6aR)-6-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphol-4-yl}-9H-purin-6-ylamine

(3aR,4R,6R,6aR)-4-(6-Amino-purin-9-yl)-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ<sup>5</sup>-furo[3,4-d][1,3,2]dioxaphosphole-2-thiol anion

(3aR,4R,6R,6aR)-4-(6-Amino-purin-9-yl)-6-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-oxo-tetrahydro-2λ5-furo[3,4-d][1,3,2]dioxaphosphole-2-thiol anion

Guidance literature:
With sulfur; In pyridine; for 0.0833333h;
DOI:10.1016/S0040-4039(00)00132-5
upstream raw materials:

5'-O-dimethoxytrityladenosine

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