N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester
CAS No.:446302-69-8
Molecular Formula:C₄₈H₆₇NO₁₀Si₃
Molecular Weight:902.317
Hs Code.:

N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester

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Chemical Property of N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester

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Technology Process of N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester

There total 7 articles about N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 300362-70-3
3-(3,4-bis(benzyloxy)phenethylcarbamoyl) propanoic acid

: 300362-71-4
benzyl 2,3,4-tri-O-trimethylsilyl-β-D-glucopyranoside

: 446302-69-8
N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/S0008-6215(00)00073-2

Reference yield:

: 18978-00-2
benzyl 2,3,4,6-tetra-O-trimethylsilyl-β-D-glucopyranoside

: 446302-69-8
N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetone; methanol; acetic acid / 2 h / 0 °C

2: DMAP; DCC / CH₂Cl₂ / 3 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; In methanol; dichloromethane; acetic acid; acetone; 1: Elimination / 2: Condensation;
DOI:10.1016/S0008-6215(00)00073-2

Reference yield:

: 37034-31-4
N-(tert-butoxycarbonyl)dopamine

: 446302-69-8
N-[2-(3,4-Bis-benzyloxy-phenyl)-ethyl]-succinamic acid (2R,3R,4S,5R,6R)-6-benzyloxy-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / K₂CO₃ / dimethylformamide / 24 h / 20 °C

2: 95 percent / CF₃COOH / CH₂Cl₂ / 5 h / 20 °C

3: 94 percent / pyridine / 3 h / 20 °C

4: DMAP; DCC / CH₂Cl₂ / 3 h / 20 °C

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In pyridine; dichloromethane; N,N-dimethyl-formamide; 1: Condensation / 2: Elimination / 3: Acylation / 4: Condensation;
DOI:10.1016/S0008-6215(00)00073-2