Technology Process of nickel(1+), [N,N'-(1,2-dimethyl-1,2-ethanediylidene)bis(3,3'-bis(trimethylsilyl)-[1,1'; 3',1'']terphenyl-2'-ylamine)(η3-2-propenyl)],-hexafluoroantimonate(1-)
There total 1 articles about nickel(1+), [N,N'-(1,2-dimethyl-1,2-ethanediylidene)bis(3,3'-bis(trimethylsilyl)-[1,1'; 3',1'']terphenyl-2'-ylamine)(η3-2-propenyl)],-hexafluoroantimonate(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
diethyl ether;
byproducts: AgCl; under Ar; a ligand (0.24 mmol), Ni-contg. compd. (0.12 mmol), and Ag-contg. compd. (0.24 mmol) in ethyl ether were stirred at room temp. for 12 h; the mixt. was filtered and the solvent was evapd. in vac.; the residue was washed with pentane and dried; recrystn. from toluene; elem. anal.;
DOI:10.1016/j.jorganchem.2004.01.003
