Cyclo-3-nitro-L-tyrosyl-L-proline

Base Information

Chemical Name:Cyclo-3-nitro-L-tyrosyl-L-proline
CAS No.:125034-08-4
Molecular Formula:C₁₄H₁₅N₃O₅
Molecular Weight:305.29
Hs Code.:

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Chemical Property of Cyclo-3-nitro-L-tyrosyl-L-proline

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Technology Process of Cyclo-3-nitro-L-tyrosyl-L-proline

There total 4 articles about Cyclo-3-nitro-L-tyrosyl-L-proline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 128404-28-4
3-nitro-L-tyrosyl-L-proline methyl ester hydrochloride

: 125034-08-4
Cyclo-3-nitro-L-tyrosyl-L-proline

Guidance literature:: With 4-methyl-morpholine; acetic acid; In iso-butanol; Heating;

Reference yield:

: 5575-03-1
(2S)-2-tert-butoxycarbonylamino-3-(4-hydroxy-3-nitro-phenyl)-propionic acid

: 125034-08-4
Cyclo-3-nitro-L-tyrosyl-L-proline

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / 1-hydroxybenzotriazole, N-methylmorpholine, N,N'-dicyclohexylcarbodiimide / dimethylformamide; CH₂Cl₂ / 1) 0-5 deg C, 2) 20 deg C

2: 89 percent / 4N hydrogen chloride / dioxane

3: 50 percent / N-methylmorpholine, acetic acid / butan-2-ol / Heating

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; iso-butanol;

Reference yield:

: 2577-48-2
methyl (2S)-pyrrolidine carboxylate

: 125034-08-4
Cyclo-3-nitro-L-tyrosyl-L-proline

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / 1-hydroxybenzotriazole, N-methylmorpholine, N,N'-dicyclohexylcarbodiimide / dimethylformamide; CH₂Cl₂ / 1) 0-5 deg C, 2) 20 deg C

2: 89 percent / 4N hydrogen chloride / dioxane

3: 50 percent / N-methylmorpholine, acetic acid / butan-2-ol / Heating

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; iso-butanol;