diphenylborylferrocene

Base Information

Chemical Name:diphenylborylferrocene
CAS No.:181149-08-6
Molecular Formula:C₂₂H₁₉BFe
Molecular Weight:350.051
Hs Code.:

Synonyms:

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Chemical Property of diphenylborylferrocene

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Technology Process of diphenylborylferrocene

There total 2 articles about diphenylborylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1-(chloromercuri)ferrocene

: 5123-17-1
bromodiphenylborane

: 181149-08-6
diphenylborylferrocene

Guidance literature:: In hexane; (N2, Schlenk technique); addn. of hexane soln. of boron compd. to suspn.of iron compd. in hexane at -78°C, warming to room temp., stirri ng overnight; filtration, concg., isolation of crystals, elem. anal.;
DOI:10.1039/b821406a

Reference yield: 62.0%

: 1271-15-4
lithiumferrocene

: 13471-36-8
methyl diphenylborinate

: 181149-08-6
diphenylborylferrocene

Guidance literature:: In hexane; byproducts: LiOMe; (argon); -78°C to room temp.; solvent removal (vac.), dissoln. (hexane), filtration, solvent removal;
DOI:10.1515/znb-1996-0615

Reference yield: 33.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 294-93-9,64491-37-8
(1,4,7,10-tetraoxacyclododecane)

: dilithioferrocene*2/3TMEDA

: 181149-08-6
diphenylborylferrocene

: [Li(12-crown-4)(THF)]2[(1,1'-ferrocenediyl)(B(phenyl)2(ferrocenyl))2]

Guidance literature:: In tetrahydrofuran; (N2, Schlenk technique); addn. of THF soln. of boron compd. to soln. of dilithium deriv. in THF at -78°C, warming to room temp., stirringovernight; concg., addn. of 12-crown-4 and hexane, isolation of ppt., washing with hexane, recrystn. by slow diffusion of hexane vapour to THF soln. under inert condition, elem. anal.;
DOI:10.1039/b821406a