N-{4-[10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

Base Information

• Chemical Name: N-{4-[10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine
• CAS No.: 255383-36-9
• Molecular Formula: C₄₀H₄₃N₇O₈S₂
• Molecular Weight: 813.956

Synonyms:

Chemical Property of N-{4-[10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

Chemical Property:

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Technology Process of N-{4-[10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

There total 1 articles about N-{4-[10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-{4-[7-diethoxyphosphoryl-10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1(17),13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (255383-35-8) → N-{4-[10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1(17),13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (255383-36-9)

Guidance literature:

With hydrogen bromide; In acetic acid; at 20 ℃; for 22h;

DOI:10.1021/jm901530b

Reference yield:

N-{4-[10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1(17),13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (255383-36-9) → AMD 7058 (255383-05-2)

Guidance literature:

With potassium carbonate; thiophenol; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm901530b

upstream raw materials:

N-{4-[7-diethoxyphosphoryl-10-bis(2-nitrobenzenesulfonyl)-4,7,10-triazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

Downstream raw materials:

AMD 7058

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