8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide

Base Information

• Chemical Name: 8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide
• CAS No.: 55816-37-0
• Molecular Formula: C₁₃H₁₇OP
• Molecular Weight: 220.251
• Mol file: 55816-37-0.mol

Synonyms:

Chemical Property of 8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide

There total 6 articles about 8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

8-phenyl-8-phospha-bicyclo[3.2.1]oct-6-ene 8syn-oxide (34667-08-8) → 8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide (55816-37-0)

Guidance literature:

With hydrogen; nickel; In ethanol;

DOI:10.1016/0040-4020(75)80008-1

Reference yield:

Cyclohepta-1,3-diene (876938-53-3) → 8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide (55816-37-0)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂ / Raney-Ni / ethanol

With hydrogen; nickel; In ethanol;

DOI:10.1016/0040-4020(75)80008-1

Reference yield:

6endo,7exo-dibromo-8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide (55816-49-4) → 8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide (55816-37-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Zn, AcOH / acetone

2: H₂ / Raney-Ni / ethanol

With hydrogen; acetic acid; zinc; nickel; In ethanol; acetone;

DOI:10.1016/0040-4020(75)80008-1

upstream raw materials:

8'-phenyl-spiro[[1,3]dithiolane-2,3'-(8-phospha-bicyclo[3.2.1]octane)] 8'syn-oxide

8-phenyl-8-phospha-bicyclo[3.2.1]oct-6-ene 8syn-oxide

Cyclohepta-1,3-diene

6endo,7exo-dibromo-8-phenyl-8-phospha-bicyclo[3.2.1]octane 8syn-oxide