Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester

Base Information

Chemical Name:Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester
CAS No.:1053705-24-0
Molecular Formula:C₃₁H₃₇N₈O₁₁P
Molecular Weight:728.656
Hs Code.:

Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester

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Chemical Property of Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester

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Technology Process of Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester

There total 2 articles about Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1053636-18-2
C₂₂H₂₈N₇O₅P

: 667934-39-6
2',5'-di-O-methyluridine

: 1053705-24-0
Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester

Guidance literature:: With 1H-tetrazole; In acetonitrile; at 50 ℃; for 25h;
DOI:10.1039/b500054h

Reference yield:

: 139434-75-6
N⁶-benzoyl-2',3'-O-methyleneadenosine

: 1053705-24-0
Dimethyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(6-benzoylamino-purin-9-yl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester (2R,3R,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methoxy-2-methoxymethyl-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrazole / acetonitrile / 3.67 h / 20 °C

2: tetrazole / acetonitrile / 25 h / 50 °C

With 1H-tetrazole; In acetonitrile;
DOI:10.1039/b500054h