C₁₆H₁₃⁽²⁾H₄NO₃

Base Information

• Chemical Name: C₁₆H₁₃⁽²⁾H₄NO₃
• CAS No.: 159753-90-9
• Molecular Formula: C₁₆H₁₇NO₃
• Molecular Weight: 275.284
• Mol file: 159753-90-9.mol

Synonyms:

Chemical Property of C₁₆H₁₃⁽²⁾H₄NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₃⁽²⁾H₄NO₃

There total 2 articles about C₁₆H₁₃⁽²⁾H₄NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<2',3',5',6'-2H4>-L-tyrosine (62595-14-6) + benzyl alcohol (100-51-6,185532-71-2) → C16H13(2)H4NO3 (159753-90-9)

Guidance literature:

With toluene-4-sulfonic acid; at 100 ℃;

DOI:10.1002/jlcr.2580340905

Reference yield:

phenol-d6 (13127-88-3,80441-87-8) → C16H13(2)H4NO3 (159753-90-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / aq. ammonium acetate, sodium sulfite, EDTA, pyridoxal phosphate, NaOH / 20 h / 37 °C / cells of Erwinia herbicola

2: p-toluenesulfonic acid / 100 °C

With ammonium acetate; sodium hydroxide; ethylenediaminetetraacetic acid; pyridoxal 5'-phosphate; toluene-4-sulfonic acid; sodium sulfite;

DOI:10.1002/jlcr.2580340905

Reference yield:

C16H13(2)H4NO3 (159753-90-9) → C9H7(2)H4NO2 (54793-54-3)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / Heating

2: H₂ / 10percent Pd/C / ethanol / 24 h / 3800 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; acetone;

DOI:10.1002/jlcr.2580340905

upstream raw materials:

<2',3',5',6'-2H4>-L-tyrosine

benzyl alcohol

phenol-d6

Downstream raw materials:

C₉H₇⁽²⁾H₄NO₂

Refernces