bis(pentacarbonyl)chrom-μ-diisocyanodiphenylmethan

Base Information

• Chemical Name: bis(pentacarbonyl)chrom-μ-diisocyanodiphenylmethan
• CAS No.: 100852-21-9
• Molecular Formula: C₂₅H₁₀Cr₂N₂O₁₀
• Molecular Weight: 602.354
• Mol file: 100852-21-9.mol

Synonyms:

Chemical Property of bis(pentacarbonyl)chrom-μ-diisocyanodiphenylmethan

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of bis(pentacarbonyl)chrom-μ-diisocyanodiphenylmethan

There total 1 articles about bis(pentacarbonyl)chrom-μ-diisocyanodiphenylmethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

aluminum bromide + ((CO)5CrCNC(C6H5)2)(1+)*AlBr4(1-)=(CO)5CrCNC(C6H5)2AlBr4 → bis(pentacarbonyl)chrom-μ-diisocyanodiphenylmethan (100852-21-9)

Guidance literature:

In dichloromethane; under N2; -10°C; after 90 min cooling at -20°C; addn. of THF;; filtered; solvent removed in vac.; recrystd. from pentane/diethyl ether; dried in vac. at 0°C; elem.anal.;;

DOI:10.1016/0022-328X(85)87303-4