6,7-Dimethoxyphthalazine

Base Information

Chemical Name:6,7-Dimethoxyphthalazine
CAS No.:13705-95-8
Molecular Formula:C10H10N2O2
Molecular Weight:190.19900
Hs Code.:
DSSTox Substance ID:DTXSID70423489
Wikidata:Q82235720
ChEMBL ID:CHEMBL1575695
Mol file:13705-95-8.mol

Synonyms:6,7-dimethoxyphthalazine;13705-95-8;HMS2414B20;SMR000115152;MLS000549190;SCHEMBL9549005;CHEMBL1575695;DTXSID70423489;AM-944/40948025

Suppliers and Price of 6,7-Dimethoxyphthalazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
6,7-DIMETHOXYPHTHALAZINE 95.00%
5MG
$ 499.13

Total 0 raw suppliers

Chemical Property of 6,7-Dimethoxyphthalazine

Chemical Property:

PSA：44.24000
LogP:1.64700
XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:190.074227566
Heavy Atom Count:14
Complexity:169

Purity/Quality:: 6,7-DIMETHOXYPHTHALAZINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C2C=NN=CC2=C1)OC

Technology Process of 6,7-Dimethoxyphthalazine

There total 4 articles about 6,7-Dimethoxyphthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.4%

: 43073-12-7
4,5-dimethoxy-phthalaldehyde

: 13705-95-8
6,7-dimethoxyphthalazine

Guidance literature:: With hydrazine hydrate; In ethanol; for 5h; Heating;
DOI:10.1002/jps.2600690140

Reference yield:

: 103477-58-3
2-(2-bromo-4,5-dimethoxyphenyl)-1,3-dioxolane

: 13705-95-8
6,7-dimethoxyphthalazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / -78 - -40 °C

1.2: 1 h / -78 °C

2.1: water / acetone / 1 h

3.1: hydrazine / ethanol / 3 h / 0 - 23 °C

With n-butyllithium; water; hydrazine; In tetrahydrofuran; ethanol; acetone;
DOI:10.1515/hc-2012-0079

Reference yield:

: 132628-76-3
2-(1,3-dioxolan-2-yl)-4,5-dimethoxybenzaldehyde

: 13705-95-8
6,7-dimethoxyphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: water / acetone / 1 h

2: hydrazine / ethanol / 3 h / 0 - 23 °C

With water; hydrazine; In ethanol; acetone;
DOI:10.1515/hc-2012-0079