cis-1-benzyl-3-benzyl-4-methylazetidinone

Base Information

• Chemical Name: cis-1-benzyl-3-benzyl-4-methylazetidinone
• CAS No.: 103776-32-5
• Molecular Formula: C₁₈H₁₉NO
• Molecular Weight: 265.355
• Mol file: 103776-32-5.mol

Synonyms:

Chemical Property of cis-1-benzyl-3-benzyl-4-methylazetidinone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-1-benzyl-3-benzyl-4-methylazetidinone

There total 3 articles about cis-1-benzyl-3-benzyl-4-methylazetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H28NO3PS2*C6H15N → cis-1-benzyl-3-benzyl-4-methylazetidinone (103776-32-5)

Guidance literature:

With triethylamine; In dichloromethane; at 25 - 30 ℃;

DOI:10.1246/bcsj.79.1748

Reference yield:

2-benzyl-3-benzylamino-butyric acid → cis-1-benzyl-3-benzyl-4-methylazetidinone (103776-32-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / triphenylphosphine / CH₂Cl₂ / 24 h / 25 - 30 °C

2: triethylamine / CH₂Cl₂

With triethylamine; triphenylphosphine; In dichloromethane;

DOI:10.1246/bcsj.79.1748

Reference yield:

S-1,3-benzothiazol-2-yl 2-benzyl-3-(benzylamino)butanethioate → cis-1-benzyl-3-benzyl-4-methylazetidinone (103776-32-5)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1246/bcsj.79.1748