[RuH(κ2-O2CCF3)(=C=CH2)(PCy3)2]

Base Information

Chemical Name:[RuH(κ2-O2CCF3)(=C=CH2)(PCy3)2]
CAS No.:855921-71-0
Molecular Formula:C₄₀H₆₉F₃O₂P₂Ru
Molecular Weight:801.999
Hs Code.:

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Chemical Property of [RuH(κ2-O2CCF3)(=C=CH2)(PCy3)2]

Chemical Property:

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Technology Process of [RuH(κ2-O2CCF3)(=C=CH2)(PCy3)2]

There total 1 articles about [RuH(κ2-O2CCF3)(=C=CH2)(PCy3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 209330-49-4
[RuHCl(CCH₂)(P(C₆H₁₁)3)2]

: 2923-16-2
potassium trifluoroacetate

: 855921-71-0
[RuH(κ2-O2CCF3)(=C=CH2)(PCy3)2]

Guidance literature:: In tetrahydrofuran; byproducts: KCl; Ar atm.; soln. of Ru complex in THF treated with CF3CO2K, stirred at room temp. for 10 min; evapd. under vac., residue extd. with toluene, extract evapd. to drynessunder vac., solid washed with pentane, dried under vac.; elem. anal.;
DOI:10.1039/b502440d

Reference yield: 94.0%

: 855921-71-0
[RuH(κ2-O2CCF3)(=C=CH2)(PCy3)2]

: 76-05-1
trifluoroacetic acid

: [Ru(O₂CCF₃)2(CHCH₃)(P(C₆H₁₁)3)2]

Guidance literature:: In tetrahydrofuran; Ar atm.; soln. of CF3COOH in THF added dropwise to soln. of Ru complex in THF at -78°C, mixt. warmed to room temp., stirred for 10 min; evapd. under vac., residue washed twice with methanol and dried under vac.; elem. anal.;
DOI:10.1039/b502440d