bis[5-(4'-tert-butyl)benzoylamino-8-hydroxyquinolinate]zinc(II) dihydrate

Base Information

Chemical Name:bis[5-(4'-tert-butyl)benzoylamino-8-hydroxyquinolinate]zinc(II) dihydrate
CAS No.:667465-58-9
Molecular Formula:C₄₀H₄₂N₄O₆Zn
Molecular Weight:740.187
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[5-(4'-tert-butyl)benzoylamino-8-hydroxyquinolinate]zinc(II) dihydrate

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Technology Process of bis[5-(4'-tert-butyl)benzoylamino-8-hydroxyquinolinate]zinc(II) dihydrate

There total 1 articles about bis[5-(4'-tert-butyl)benzoylamino-8-hydroxyquinolinate]zinc(II) dihydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 667465-52-3
5-(4'-tert-butyl)-benzoylamino-8-hydroxyquinoline hydrochloride

: 7732-18-5
water

: 7646-85-7,24359-56-6
zinc(II) chloride

: 667465-58-9
bis[5-(4'-tert-butyl)benzoylamino-8-hydroxyquinolinate]zinc(II) dihydrate

Guidance literature:: With ammonium acetate; In methanol; water; a hot soln. of a ligand (0.419 mmol) in MeOH was added dropwise to a stirred soln. contg. ZnCl2 (0.209 mmol) and ammonium acetate (6.075 mmol) dissolved in H2O; stirring for 5 h; solid was filtered off, washed with water and methanol, filtered and dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(03)00427-4