Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester

Base Information

Chemical Name:Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester
CAS No.:127221-62-9
Molecular Formula:C₄₆H₅₃N₂O₁₃P
Molecular Weight:872.906
Hs Code.:

Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester

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Chemical Property of Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester

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Technology Process of Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester

There total 4 articles about Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82231-40-1,82231-43-4
(2S,3S,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-(2-benzyloxy-ethoxy)-6-benzyloxymethyl-tetrahydro-pyran

: 127221-62-9
Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd-C

2: 67 percent / CCl₃CN / pyridine / 80 °C

3: triisopropylbenzenesulfonyl-triazole (TPSNT) / pyridine

With triisopropylbenzenesulfonyl-triazole; hydrogen; trichloroacetonitrile; palladium on activated charcoal; In pyridine;
DOI:10.1016/S0040-4039(01)93843-2

Reference yield:

: 148905-25-3
2,3,4,6-tetra-O-benzyl-D-mannopyranosyl bromide

: 127221-62-9
Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Hg(CN)2 / nitromethane

2: H₂ / Pd-C

3: 67 percent / CCl₃CN / pyridine / 80 °C

4: triisopropylbenzenesulfonyl-triazole (TPSNT) / pyridine

With triisopropylbenzenesulfonyl-triazole; hydrogen; mercury(II) cyanide; trichloroacetonitrile; palladium on activated charcoal; In pyridine; nitromethane;
DOI:10.1016/S0040-4039(01)93843-2

Reference yield:

: 852395-47-2
hydroxyethyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside

: 127221-62-9
Phosphoric acid (2S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester 2-((2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / CCl₃CN / pyridine / 80 °C

2: triisopropylbenzenesulfonyl-triazole (TPSNT) / pyridine

With triisopropylbenzenesulfonyl-triazole; trichloroacetonitrile; In pyridine;
DOI:10.1016/S0040-4039(01)93843-2