Technology Process of C15H21F2NO4
There total 6 articles about C15H21F2NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: diethyl ether / 0.5 h / 0 °C
2: hydrogen bromide / tetrahydrofuran; water / 1 h / 0 °C
3: potassium fluoride / N,N-dimethyl-formamide / 1 h / 20 °C
4: sodium tetrahydroborate / ethanol / 0.5 h / 0 °C
5: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C
With
potassium fluoride; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen bromide; hydrogen;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;
3: modified Finkel-stein reaction;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen bromide / tetrahydrofuran; water / 1 h / 0 °C
2: potassium fluoride / N,N-dimethyl-formamide / 1 h / 20 °C
3: sodium tetrahydroborate / ethanol / 0.5 h / 0 °C
4: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C
With
potassium fluoride; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen bromide; hydrogen;
In
tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
2: modified Finkel-stein reaction;