OsCl(CO)(P(C₆H₅)3)2(SeCC₆H₄CH₃)

Base Information

• Chemical Name: OsCl(CO)(P(C₆H₅)3)2(SeCC₆H₄CH₃)
• CAS No.: 75346-83-7
• Molecular Formula: C₄₅H₃₇ClOOsP₂Se
• Molecular Weight: 960.349

Synonyms:

Chemical Property of OsCl(CO)(P(C₆H₅)3)2(SeCC₆H₄CH₃)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of OsCl(CO)(P(C₆H₅)3)2(SeCC₆H₄CH₃)

There total 3 articles about OsCl(CO)(P(C₆H₅)3)2(SeCC₆H₄CH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

selenium (7782-49-2) + OsCl(CC6H4CH3)(CO)(P(C6H5)3)2 → OsCl(CO)(P(C6H5)3)2(SeCC6H4CH3) (75346-83-7)

Guidance literature:

In benzene; stirred for 2,5h; filtered through a celite pad, ethanol added, solvent volume lowered under reduced pressure, crystd., collected, recrystd. from CH2Cl2/ethanol,elem. anal.;

DOI:10.1016/0022-328X(86)80439-9

Reference yield: 33.0%

sodium hydrogen selenide + OsCl2(CO)(P(C6H5)3)2(C(Cl)C6H4CH3) → OsCl(CO)(P(C6H5)3)2(SeCC6H4CH3) (75346-83-7)

Guidance literature:

In dichloromethane; complex dissolved, NaSeH soln. added, stirred for 1 min; hexane added, solvent volume lowered under reduced pressure, collected,chromd. (silica gel, CH2Cl2), ethanol added, CH2Cl2 removed under reduced pressure, crystd.;

DOI:10.1016/0022-328X(86)80439-9

Reference yield:

hydrogen seleinde + OsCl2(CO)(P(C6H5)3)2(C(Cl)C6H4CH3) → OsCl(CO)(P(C6H5)3)2(SeCC6H4CH3) (75346-83-7)

Guidance literature:

In not given; elem. anal.;

DOI:10.1021/ja00541a038

upstream raw materials:

selenium

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