C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-)

Base Information

Chemical Name:C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-)
CAS No.:134028-79-8
Molecular Formula:C₄₉H₆₈O₆PSi*Cl
Molecular Weight:847.588
Hs Code.:

C<sub>49</sub>H<sub>68</sub>O<sub>6</sub>PSi<sup>(1+)</sup>*Cl<sup>(1-)</sup>

Synonyms:

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Chemical Property of C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-)

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Technology Process of C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-)

There total 3 articles about C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 134004-77-6
2,2-Dimethyl-butyric acid (1R,5S,6R,8S,9S,10S,11S)-10-{2-[(2R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-6-oxo-tetrahydro-pyran-2-yl]-ethyl}-6,11-dimethyl-3,3,3-triphenyl-2,4-dioxa-3λ⁵-phospha-tricyclo[7.4.0.0^1,5]tridec-8-yl ester

: 134004-70-9
2,2-Dimethyl-butyric acid (1S,7S,8S,8aR)-8-{2-[(2R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-6-oxo-tetrahydro-pyran-2-yl]-ethyl}-3,7-dimethyl-1,2,6,7,8,8a-hexahydro-naphthalen-1-yl ester

: 134028-79-8
C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-)

: 127343-16-2
6(R)-<2-<8(S)-<(2,2-dimethylbutyryl)oxy>-2(S),6(R)-dimethyl-5-oxo-1,2,3,4,5,6,7,8,8a(R)-nonahydronaphtyl-1(S)>ethyl>-4(R)-<(tert-butyldimethylsilyl)oxy>-3,4,5,6-tetrahydro-2H-pyran-2-one

Guidance literature:: for 16h;
DOI:10.1021/jo00011a022

Reference yield:

: 127343-13-9
6(R)-<2-<8(S)-<(2,2-dimethylbutyryl)oxy>-2(S),6(R)-dimethyl-1,2,3,4,6,7,8,8a(R)-octahydronaphthyl-1(S)>ethyl>-4(R)-<(tert-butyldimethylsilyl)oxy>-3,4,5,6-tetrahydro-2H-pyran-2-one

: 134028-79-8
C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / H₂O, trimethylamine N-oxide dihydrate, pyridine, OsO₄ / acetone / 18 h / 60 - 62 °C

2: diisopropylethylamine / CD₃CN / 3.5 h / Ambient temperature

3: 27 percent / 16 h

With pyridine; osmium(VIII) oxide; trimethylamine-N-oxide; water; N-ethyl-N,N-diisopropylamine; In [D₃]acetonitrile; acetone;
DOI:10.1021/jo00011a022

Reference yield:

: 134004-76-5
6(R)-<2-<8(S)-<(2,2-dimethylbutyryl)oxy>-4a(R),5(S)-dihydroxy-2(S),6(R)-dimethyl-1,2,3,4,4a,5,6,7,8,8a(R)-decahydronaphth-1(S)-yl>ethyl>-4(R)-(tert-butyldimethylsiloxy)-3,4,5,6-tetrahydro-2H-pyran-2-one

: 134028-79-8
C₄₉H₆₈O₆PSi⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropylethylamine / CD₃CN / 3.5 h / Ambient temperature

2: 27 percent / 16 h

With N-ethyl-N,N-diisopropylamine; In [D₃]acetonitrile;
DOI:10.1021/jo00011a022