C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-)

Base Information

Chemical Name:C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-)
CAS No.:1319713-09-1
Molecular Formula:C₁₇H₁₄ClNP*Cl
Molecular Weight:334.185
Hs Code.:

C<sub>17</sub>H<sub>14</sub>ClNP<sup>(1+)</sup>*Cl<sup>(1-)</sup>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-)

Chemical Property:

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Technology Process of C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-)

There total 2 articles about C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64741-30-6
2-(diphenylphosphoryl)pyridine

: 1319713-09-1
C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-)

Guidance literature:: With oxalyl dichloride; In chloroform-d1; for 0.5h;
DOI:10.1021/jo201085r

Reference yield:

: 37943-90-1
2-(diphenylphosphino)pyridine

: 1319713-09-1
C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / tetrahydrofuran; water / 0.53 h

2: oxalyl dichloride / chloroform-d1 / 0.5 h

With oxalyl dichloride; dihydrogen peroxide; In tetrahydrofuran; chloroform-d1; water;
DOI:10.1021/jo201085r

Reference yield:

: 75-84-3
2,2-dimethyl-propanol-1

: 1319713-09-1
C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-)

: 120711-44-6
C₂₇H₃₆NO₂P

Guidance literature:: 2,2-dimethyl-propanol-1; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 0.0166667h; Inert atmosphere; Schlenk technique;

C₁₇H₁₄ClNP⁽¹⁺⁾*Cl^(1-); In diethyl ether; hexane; at -78 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4cc02171a