Technology Process of C9H14(2)H2O
There total 5 articles about C9H14(2)H2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium deuteride;
In
diethyl ether;
Yield given;
from -40 to 0 degC over 1 h;
DOI:10.1002/recl.19881070304
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 83 percent / sodium hydride / diethyl ether / 5 h reflux, overnight at room t.
2: stannic chloride / CH2Cl2 / Ambient temperature
3: 100 percent / sodium borohydride / ethanol; H2O / 4 h / Ambient temperature
4: 58 percent / POCl3 / pyridine / 22 h / 95 °C
5: LiAlD4 / diethyl ether / from -40 to 0 degC over 1 h
With
sodium tetrahydroborate; lithium aluminium deuteride; tin(IV) chloride; sodium hydride; trichlorophosphate;
In
pyridine; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1002/recl.19881070304
- Guidance literature:
-
Multi-step reaction with 4 steps
1: stannic chloride / CH2Cl2 / Ambient temperature
2: 100 percent / sodium borohydride / ethanol; H2O / 4 h / Ambient temperature
3: 58 percent / POCl3 / pyridine / 22 h / 95 °C
4: LiAlD4 / diethyl ether / from -40 to 0 degC over 1 h
With
sodium tetrahydroborate; lithium aluminium deuteride; tin(IV) chloride; trichlorophosphate;
In
pyridine; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1002/recl.19881070304