C₆₁H₈₀F₅N₅O₁₆

Base Information

Chemical Name:C₆₁H₈₀F₅N₅O₁₆
CAS No.:148914-68-5
Molecular Formula:C₆₁H₈₀F₅N₅O₁₆
Molecular Weight:1234.32
Hs Code.:

C<sub>61</sub>H<sub>80</sub>F<sub>5</sub>N<sub>5</sub>O<sub>16</sub>

Synonyms:

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Chemical Property of C₆₁H₈₀F₅N₅O₁₆

Chemical Property:

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Technology Process of C₆₁H₈₀F₅N₅O₁₆

There total 24 articles about C₆₁H₈₀F₅N₅O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19728-63-3
N-benzyloxycarbonyl-L-treonine

: 148914-68-5,148969-36-2
C₆₁H₈₀F₅N₅O₁₆

Guidance literature:: Multi-step reaction with 9 steps

1: 75 percent / NEt₃ / ethyl acetate / 48 h / 20 °C

2: 98 percent / dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 15 h / -30 deg C -> 20 deg C

3: 88 percent / 5 N HCl / dioxane / 2 h / 20 °C

4: 93 percent / 1 N NaHCO₃ / CHCl₃

5: 95 percent / N,N-bis<2-oxo-3-oxazolidinyl>phosphorodiamidic chloride, N-ethyldiisopropylamine / CH₂Cl₂ / 15 h / 0 deg C -> 20 deg C

6: 95 percent / Zn-powder, 90 percent aq. AcOH / 20 °C

7: 70 percent / N,N-bis<2-oxo-3-oxazolidinyl>phosphorodiamidic chloride, N-ethyldiisopropylamine / CH₂Cl₂ / 15 h / 0 deg C -> room temperature

8: 100 percent / Zn-powder, 90 percent aq. AcOH / 15 h / 20 °C

9: dicyclohexylcarbodiimide / CH₂Cl₂ / 15 h / -20 deg C -> 20 deg C

With hydrogenchloride; N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; sodium hydrogencarbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; zinc; dmap; In 1,4-dioxane; dichloromethane; chloroform; ethyl acetate;
DOI:10.1055/s-1991-26448

Reference yield:

: 118878-51-6,118878-52-7
MCA-(2RS,4S)-Hip-OH

: 148914-68-5,148969-36-2
C₆₁H₈₀F₅N₅O₁₆

Guidance literature:: Multi-step reaction with 8 steps

1: 88 percent / triethylamine, dicyclohexylcarbodiimide / CH₂Cl₂ / 20 h / 0 deg C -> 20 deg C

2: 78 percent / N,N-pentamethylenethiourea, triethylamine / dioxane / 3 h / 70 °C

3: 95 percent / dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 20 h / -20 deg C -> 20 deg C

4: 50 percent aq. HF / acetonitrile / 15 h / 20 °C

5: 6 N HCl / dioxane / 1 h / 20 °C

6: 70 percent / N,N-bis<2-oxo-3-oxazolidinyl>phosphorodiamidic chloride, N-ethyldiisopropylamine / CH₂Cl₂ / 15 h / 0 deg C -> room temperature

7: 100 percent / Zn-powder, 90 percent aq. AcOH / 15 h / 20 °C

8: dicyclohexylcarbodiimide / CH₂Cl₂ / 15 h / -20 deg C -> 20 deg C

With hydrogenchloride; N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; hydrogen fluoride; piperidine-1-carbothioamide; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; zinc; dmap; In 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1055/s-1991-26448

Reference yield:

: 135103-20-7,135214-06-1
MCA-(2RS,4S)-Hip-Leu-OTCE

: 148914-68-5,148969-36-2
C₆₁H₈₀F₅N₅O₁₆

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent / N,N-pentamethylenethiourea, triethylamine / dioxane / 3 h / 70 °C

2: 95 percent / dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 20 h / -20 deg C -> 20 deg C

3: 50 percent aq. HF / acetonitrile / 15 h / 20 °C

4: 6 N HCl / dioxane / 1 h / 20 °C

5: 70 percent / N,N-bis<2-oxo-3-oxazolidinyl>phosphorodiamidic chloride, N-ethyldiisopropylamine / CH₂Cl₂ / 15 h / 0 deg C -> room temperature

6: 100 percent / Zn-powder, 90 percent aq. AcOH / 15 h / 20 °C

7: dicyclohexylcarbodiimide / CH₂Cl₂ / 15 h / -20 deg C -> 20 deg C

With hydrogenchloride; N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; hydrogen fluoride; piperidine-1-carbothioamide; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; zinc; dmap; In 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1055/s-1991-26448