B₁₀H₁₂(P(CH₃)2(C₆H₅))2

Base Information

Chemical Name:B₁₀H₁₂(P(CH₃)2(C₆H₅))2
CAS No.:101943-92-4
Molecular Formula:C₁₆H₃₄B₁₀P₂
Molecular Weight:396.503
Hs Code.:

B<sub>10</sub>H<sub>12</sub>(P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>))2

Synonyms:

Suppliers and Price of B₁₀H₁₂(P(CH₃)2(C₆H₅))2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of B₁₀H₁₂(P(CH₃)2(C₆H₅))2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of B₁₀H₁₂(P(CH₃)2(C₆H₅))2

There total 2 articles about B₁₀H₁₂(P(CH₃)2(C₆H₅))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 17702-41-9
nido-decaborane

: 672-66-2
Dimethyl(phenyl)phosphine

: 101943-92-4,110201-15-5,110222-20-3
B₁₀H₁₂(P(CH₃)2(C₆H₅))2

Guidance literature:: In tetrahydrofuran; (N2); dissoln. of B10H14 in THF, cooling to ca. 200 K, addn. of PMe2Ph, stirring 15 min at low temp. and 2 h at room temp.; removal of volatiles, dissoln. (CH2Cl2), repeated prep. TLC (SiO2; CH2Cl2/hexane) delivers the exo/exo- and exo/endo-arachno compd.;

Reference yield:

: 28377-92-6
bis(dimethyl sulfide) arachno-decaborane⁽¹⁴⁾

: 672-66-2
Dimethyl(phenyl)phosphine

: 101943-92-4,110201-15-5,110222-20-3
B₁₀H₁₂(P(CH₃)2(C₆H₅))2

Guidance literature:: In ⁽²⁾H₈-toluene; byproducts: S(CH3)2; treating of exo,exo-6,9-(SMe2)2B10H12 with a stoich. amt. of PMe2Ph in CD2Cl2 soln. at ca. 203 K for 24 h under dry N2; mixt. of endo,exo-6,9 and exo,exo-6,9 isomers was obtained; detected by n.m.r.;