C₅₁H₇₆O₁₄SSi

Base Information

Chemical Name:C₅₁H₇₆O₁₄SSi
CAS No.:138213-60-2
Molecular Formula:C₅₁H₇₆O₁₄SSi
Molecular Weight:973.308
Hs Code.:

C<sub>51</sub>H<sub>76</sub>O<sub>14</sub>SSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₁H₇₆O₁₄SSi

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Technology Process of C₅₁H₇₆O₁₄SSi

There total 9 articles about C₅₁H₇₆O₁₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138194-37-3
(E)-(2S,3S,5S)-8-(1-Ethoxy-ethoxy)-2-methoxymethoxy-3,5,7-trimethyl-oct-6-en-1-ol

: 138213-60-2
C₅₁H₇₆O₁₄SSi

Guidance literature:: Multi-step reaction with 8 steps

1: 92 percent / N-methylmorpholine-N-oxide, MS 4A, / n-Pr₄NRuO₄ / CH₂Cl₂ / Ambient temperature

3: 1) t-BuLi / 1) THF, -80 deg C, 1h, 2) -80 to 0 deg C, 4h

4: 81 percent / NMO, MS 4A / n-Pr₄RuO₄ / acetonitrile / 5 h

5: aq. HF / acetonitrile / 1.17 h / Ambient temperature

6: N-chlorosuccinimide, Me₂S / CH₂Cl₂ / 0 °C

7: dimethylformamide / 12 h / Ambient temperature

8: PPTS / 12 h / Ambient temperature

With N-chloro-succinimide; N-methyl-2-indolinone; dimethylsulfide; hydrogen fluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate; n-Pr₄RuO₄; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)93498-1

Reference yield:

: (E)-(2S,3S,5S)-8-(1-Ethoxy-ethoxy)-2-methoxymethoxy-3,5,7-trimethyl-oct-6-enal

: 138213-60-2
C₅₁H₇₆O₁₄SSi

Guidance literature:: Multi-step reaction with 7 steps

2: 1) t-BuLi / 1) THF, -80 deg C, 1h, 2) -80 to 0 deg C, 4h

3: 81 percent / NMO, MS 4A / n-Pr₄RuO₄ / acetonitrile / 5 h

4: aq. HF / acetonitrile / 1.17 h / Ambient temperature

5: N-chlorosuccinimide, Me₂S / CH₂Cl₂ / 0 °C

6: dimethylformamide / 12 h / Ambient temperature

7: PPTS / 12 h / Ambient temperature

With N-chloro-succinimide; N-methyl-2-indolinone; dimethylsulfide; hydrogen fluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; n-Pr₄RuO₄; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)93498-1

Reference yield:

: tert-Butyl-[(E)-(2S,3S,5S)-8-(1-ethoxy-ethoxy)-2-methoxymethoxy-3,5,7-trimethyl-oct-6-enyloxy]-dimethyl-silane

: 138213-60-2
C₅₁H₇₆O₁₄SSi

Guidance literature:: Multi-step reaction with 9 steps

1: nBu₄NF / tetrahydrofuran / Ambient temperature

2: 92 percent / N-methylmorpholine-N-oxide, MS 4A, / n-Pr₄NRuO₄ / CH₂Cl₂ / Ambient temperature

4: 1) t-BuLi / 1) THF, -80 deg C, 1h, 2) -80 to 0 deg C, 4h

5: 81 percent / NMO, MS 4A / n-Pr₄RuO₄ / acetonitrile / 5 h

6: aq. HF / acetonitrile / 1.17 h / Ambient temperature

7: N-chlorosuccinimide, Me₂S / CH₂Cl₂ / 0 °C

8: dimethylformamide / 12 h / Ambient temperature

9: PPTS / 12 h / Ambient temperature

With N-chloro-succinimide; N-methyl-2-indolinone; dimethylsulfide; hydrogen fluoride; tetrabutyl ammonium fluoride; tert.-butyl lithium; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate; n-Pr₄RuO₄; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)93498-1