[(p-cymene)Ru(NH₃)]Cl₂

Base Information

• Chemical Name: [(p-cymene)Ru(NH₃)]Cl₂
• CAS No.: 1319728-18-1
• Molecular Formula: C₁₀H₁₇Cl₂NRu
• Molecular Weight: 323.228
• Mol file: 1319728-18-1.mol

Synonyms:

Chemical Property of [(p-cymene)Ru(NH₃)]Cl₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [(p-cymene)Ru(NH₃)]Cl₂

There total 1 articles about [(p-cymene)Ru(NH₃)]Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

N,N'-dimethylbenzylamine (103-83-3) + ammonium hexafluorophosphate + [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) → [(p-cymene)Ru(NH3)]Cl2 (1319728-18-1) + (η6-p-cymene)Ru(NH3)Cl2*(N,N-dimethylbenzylammonium hexafluorophosphate)

Guidance literature:

In methanol; suspn. of ((η6-p-cym)RuCl2)2 (0.16 mmol), Me2(PhCH2)N (0.32 mmol) and NH4PF6 (0.32 mmol) in MeOH stirred under N2 at ambient temp. for 18 h; soln. evapd., solid dissolved in min. amount of MeOH, allowed to stand at 298 K for 5 h, ppt. filtered, washed with Et2O/MeOH, dried in vac. overnight; elem. anal., XRD;

DOI:10.1002/ejic.201100250

upstream raw materials:

N,N'-dimethylbenzylamine

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂