(+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide

Base Information

Chemical Name:(+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide
CAS No.:135862-16-7
Molecular Formula:C₂₉H₂₅N₅O₆S
Molecular Weight:571.613
Hs Code.:

(+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide

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Technology Process of (+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide

There total 3 articles about (+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: 135862-17-8
N-<1-<1-(phenylsulfonyl)-2-methyl-1H-indol-3-yl>vinyl>diacetamide

: 135862-16-7
(+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide

Guidance literature:: In dichloromethane; at 20 ℃; for 120h;
DOI:10.1002/hlca.19910740406

Reference yield:

: 113685-33-9
3-acetyl-2-methyl-1-(phenylsulfonyl)indole

: 135862-16-7
(+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 62.8 percent / NH₂OH*HCl, AcONa / methanol; H₂O / 20 h / Heating

2: 21 percent / pyridine / 96 h / Heating

3: 74 percent / CH₂Cl₂ / 120 h / 20 °C

With pyridine; hydroxylamine hydrochloride; sodium acetate; In methanol; dichloromethane; water;
DOI:10.1002/hlca.19910740406

Reference yield:

: 135881-95-7
(E)-1-<1-(phenylsulfonyl)-2-methyl-1H-indol-3-yl>ethanone oxime

: 135862-16-7
(+/-)-N-<2,3,11,11aβ-tetrahydro-11aβ-methyl-1,3-dioxo-2-phenyl-11-(phenylsulfonyl)-<1,2,4>triazolo<1,2-a>pyridazino<3,4-b>indol-6-yl>diacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / pyridine / 96 h / Heating

2: 74 percent / CH₂Cl₂ / 120 h / 20 °C

With pyridine; In dichloromethane;
DOI:10.1002/hlca.19910740406