AlMe₂(2,5-bis[N-(2,6-diisopropylphenyl)iminomethyl]pyrrole)

Base Information

• Chemical Name: AlMe₂(2,5-bis[N-(2,6-diisopropylphenyl)iminomethyl]pyrrole)
• CAS No.: 362631-20-7
• Molecular Formula: C₃₂H₄₄AlN₃
• Molecular Weight: 497.703
• Mol file: 362631-20-7.mol

Synonyms:

Chemical Property of AlMe₂(2,5-bis[N-(2,6-diisopropylphenyl)iminomethyl]pyrrole)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of AlMe₂(2,5-bis[N-(2,6-diisopropylphenyl)iminomethyl]pyrrole)

There total 1 articles about AlMe₂(2,5-bis[N-(2,6-diisopropylphenyl)iminomethyl]pyrrole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,5-bis{[(2,6-diisopropylphenyl)imino]methyl}pyrrole (263547-65-5) + trimethylaluminum (75-24-1) → AlMe2(2,5-bis[N-(2,6-diisopropylphenyl)iminomethyl]pyrrole) (362631-20-7)

Guidance literature:

In toluene; byproducts: CH4; under Ar atm. using Schlenk techniques; to soln. of pyrrole in toluene added soln. of AlMe3 in toluene at -78°C; after evolution of CH4 gas was completed, mixt. allowed to warm to room temp.; stirred for 6 h at room temp.; volatiles removed (vac.); recrystd. (THF-hexane); elem. anal.;

DOI:10.1246/bcsj.76.1965

upstream raw materials:

2,5-bis{[(2,6-diisopropylphenyl)imino]methyl}pyrrole

trimethylaluminum