tetra(mesityl)oxalamidine(triphenylphosphine)copper(I) tetrafluoroborate

Base Information

Chemical Name:tetra(mesityl)oxalamidine(triphenylphosphine)copper(I) tetrafluoroborate
CAS No.:723312-48-9
Molecular Formula:BF₄*C₅₆H₆₁CuN₄P
Molecular Weight:971.452
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetra(mesityl)oxalamidine(triphenylphosphine)copper(I) tetrafluoroborate

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Technology Process of tetra(mesityl)oxalamidine(triphenylphosphine)copper(I) tetrafluoroborate

There total 1 articles about tetra(mesityl)oxalamidine(triphenylphosphine)copper(I) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 286476-84-4
tetra(mesityl)oxalic amidine

: 603-35-0
triphenylphosphine

: 723312-48-9
tetra(mesityl)oxalamidine(triphenylphosphine)copper(I) tetrafluoroborate

Guidance literature:: In toluene; all manipulations under Ar; suspn. of Cu complex and oxalamidine in toluene stirred for 20 min, soln. of PPh3 in toluene added dropwise, heated under reflux for 4 h; concd., n-hexane added dropwise until crystn. started, stored at -25°C for 12 h, ppt. filtered off, washed with n-hexane, dried under vac.; elem. anal.;
DOI:10.1002/zaac.200300181