(5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid

Base Information

Chemical Name:(5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid
CAS No.:77931-56-7
Molecular Formula:C₂₂H₃₂Cl₂N₂O₄
Molecular Weight:459.413
Hs Code.:

(5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4-<di-(2-chloroethyl)amino>-phenylacetic acid

Synonyms:

Suppliers and Price of (5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid

There total 3 articles about (5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1670-47-9
1,1-diethoxycyclohexane

: 64205-65-8
(2-Hydroxymethyl-1,3-dihydroxy-2-propyl)amide of 4-phenylacetic acid

: 77931-56-7
(5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid

Guidance literature:: toluene-4-sulfonic acid; Heating;
DOI:10.1007/BF00758456

Reference yield:

: 10477-72-2
4-bis(2-chloroethyl)aminophenylacetic acid

: 77931-56-7
(5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: 50 percent / H₂O; acetone / 0.25 h / -10 °C

3: 70 percent / p-toluenesulfonic acid / Heating

With thionyl chloride; toluene-4-sulfonic acid; In water; acetone;
DOI:10.1007/BF00758456

Reference yield:

: 53039-95-5
p-phenylacetyl chloride hydrochloride

: 77931-56-7
(5-Hydroxymethyl-2,2-pentamethylene-1,3-dioxan-5-yl)amide of 4--phenylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / H₂O; acetone / 0.25 h / -10 °C

2: 70 percent / p-toluenesulfonic acid / Heating

toluene-4-sulfonic acid; In water; acetone;
DOI:10.1007/BF00758456