1,3-Diphenyl-1H-benzoisochinolinium-hexachloroantimonat

Base Information

• Chemical Name: 1,3-Diphenyl-1H-benzoisochinolinium-hexachloroantimonat
• CAS No.: 120771-40-6
• Molecular Formula: C₂₄H₁₇N*Cl₆Sb*H
• Molecular Weight: 654.882
• Mol file: 120771-40-6.mol

Synonyms:

Chemical Property of 1,3-Diphenyl-1H-benzoisochinolinium-hexachloroantimonat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,3-Diphenyl-1H-benzoisochinolinium-hexachloroantimonat

There total 1 articles about 1,3-Diphenyl-1H-benzoisochinolinium-hexachloroantimonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-Methoxy-N-(1-naphthylphenylmethylen)benzylamin (119208-75-2) → 1,3-Diphenyl-1H-benzoisochinolinium-hexachloroantimonat (120771-40-6)

Guidance literature:

With antimonypentachloride; acetyl chloride; Yield given. Multistep reaction; 1) CHCl₃, -70 deg C, 2) CHCl₃, RT, 45 h;

Reference yield: 51.0%

1,3-Diphenyl-1H-benzoisochinolinium-hexachloroantimonat (120771-40-6) → 1,3-Diphenyl-benzo[de]isoquinolin-4-one + 1,3-Diphenyl-6H-benzoisochinolin-6-on (120742-88-3)

Guidance literature:

With potassium hydrogencarbonate; In dichloromethane; for 0.5h;

upstream raw materials:

α-Methoxy-N-(1-naphthylphenylmethylen)benzylamin

Downstream raw materials:

1,3-Diphenyl-6H-benzoisochinolin-6-on