[Ir(cyclooctadiene)(η5-cyclopentadienyl)C(CH3)2(η5-indenyl)Fe(η5-cyclopentadienyl)]

Base Information

Chemical Name:[Ir(cyclooctadiene)(η5-cyclopentadienyl)C(CH3)2(η5-indenyl)Fe(η5-cyclopentadienyl)]
CAS No.:912572-51-1
Molecular Formula:C₃₀H₃₃FeIr
Molecular Weight:641.659
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ir(cyclooctadiene)(η5-cyclopentadienyl)C(CH3)2(η5-indenyl)Fe(η5-cyclopentadienyl)]

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Technology Process of [Ir(cyclooctadiene)(η5-cyclopentadienyl)C(CH3)2(η5-indenyl)Fe(η5-cyclopentadienyl)]

There total 1 articles about [Ir(cyclooctadiene)(η5-cyclopentadienyl)C(CH3)2(η5-indenyl)Fe(η5-cyclopentadienyl)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 912572-44-2
[Ir(cyclooctadiene)(η5-cyclopentadienyl)C(CH3)2(indenyl)]

: 232282-91-6
[(cyclopentadienyl)Fe(fluorene)]PF₆

: 102-54-5,55404-68-7
ferrocene

: 912572-55-5,912572-51-1
[Ir(cyclooctadiene)(η5-cyclopentadienyl)C(CH3)2(η5-indenyl)Fe(η5-cyclopentadienyl)]

Guidance literature:: With BuLi; In tetrahydrofuran; byproducts: fluorene; (N2); (cycloctadiene)Ir(C5H4)CMe2(C9H7) deprotonated by BuLi in THF; (CpFe(fluorene)PF6 and BuLi in THF added at 0 °C after 1 h; refluxedfor 16 h; solvent removed; solid extracted by pentane/diethyl ether(1:1); fluorene and ferrocene removed by sublimation at 50 °C; residue filtered through Al2O3 column with pentane; eluted (pentane/diethyl ether); elem. anal.;
DOI:10.1002/zaac.200500229