closo-3-(PPh3)-3-(η2-CH3CO2)-1,2-(μ-(CH2)3)-3,1,2-RhC2B9H9

Base Information

Chemical Name:closo-3-(PPh3)-3-(η2-CH3CO2)-1,2-(μ-(CH2)3)-3,1,2-RhC2B9H9
CAS No.:127943-61-7
Molecular Formula:C₂₅H₃₃B₉O₂PRh
Molecular Weight:596.714
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of closo-3-(PPh3)-3-(η2-CH3CO2)-1,2-(μ-(CH2)3)-3,1,2-RhC2B9H9

Chemical Property:

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Technology Process of closo-3-(PPh3)-3-(η2-CH3CO2)-1,2-(μ-(CH2)3)-3,1,2-RhC2B9H9

There total 1 articles about closo-3-(PPh3)-3-(η2-CH3CO2)-1,2-(μ-(CH2)3)-3,1,2-RhC2B9H9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 108-22-5
Isopropenyl acetate

: {closo-3,3-(PPh₃)2-3-D-3,1,2-RhC₂B₉H₁₁}

: 127943-61-7
closo-3-(PPh3)-3-(η2-CH3CO2)-1,2-(μ-(CH2)3)-3,1,2-RhC2B9H9

Guidance literature:: In benzene; Ar-atmosphere; stirring (25°C, 3 d); filtration, partial evapn., heptane addn., partial evapn., cooling (overnight), collection, washing (pentane), recrystn. (benzene/heptane and CH2Cl2/heptane); elem. anal.;

Reference yield:

: 617-86-7
triethylsilane

: 127943-61-7
closo-3-(PPh3)-3-(η2-CH3CO2)-1,2-(μ-(CH2)3)-3,1,2-RhC2B9H9

: 127916-00-1
exo-nido-(PPh3)2Rh-7,8-(μ-(CH2)3)-7,8-C2B9H10

Guidance literature:: With triphenylphosphine; In dichloromethane; dichloromethane-d2; Ar-atmosphere; 40°C, 1 d; not isolated, reaction followed by NMR spectroscopy;