[(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]⁽¹⁺⁾*B(C₆F₅)4^(1-)=[(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]B(C₆F₅)4

Base Information

• Chemical Name: [(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]⁽¹⁺⁾*B(C₆F₅)4^(1-)=[(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]B(C₆F₅)4
• CAS No.: 1013932-13-2
• Molecular Formula: C₂₄BF₂₀*C₃₃H₄₀N₄ScSi
• Molecular Weight: 1244.79
• Mol file: 1013932-13-2.mol

Synonyms:

Chemical Property of [(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]⁽¹⁺⁾*B(C₆F₅)4^(1-)=[(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]B(C₆F₅)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]⁽¹⁺⁾*B(C₆F₅)4^(1-)=[(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]B(C₆F₅)4

There total 1 articles about [(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]⁽¹⁺⁾*B(C₆F₅)4^(1-)=[(C₅H₄C(C₆H₅)2CH(N₂C₃H(CH₃)2)2)Sc(CH₂Si(CH₃)3)]B(C₆F₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

[Sc(CH2SiMe3)2(2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)] (1013932-08-5) + trityl tetrakis(pentafluorophenyl)borate → [(C5H4C(C6H5)2CH(N2C3H(CH3)2)2)Sc(CH2Si(CH3)3)](1+)*B(C6F5)4(1-)=[(C5H4C(C6H5)2CH(N2C3H(CH3)2)2)Sc(CH2Si(CH3)3)]B(C6F5)4 (1013932-13-2)

Guidance literature:

In tetrahydrofuran; byproducts: Ph3CH2SiMe3; (N2); std. Schlenk technique; soln. of Sc complex and B compd. (1 equiv.) in THF was stirred at room temp. for 30 min; evapd.; washed (hexane); filtered; dried (vac.); elem. anal.;

DOI:10.1021/om701033r

upstream raw materials:

[Sc(CH₂SiMe₃)2(2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]