C₃₂H₄₅N₇O₅S

Base Information

Chemical Name:C₃₂H₄₅N₇O₅S
CAS No.:1421639-64-6
Molecular Formula:C₃₂H₄₅N₇O₅S
Molecular Weight:639.819
Hs Code.:

C<sub>32</sub>H<sub>45</sub>N<sub>7</sub>O<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₄₅N₇O₅S

Chemical Property:

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Technology Process of C₃₂H₄₅N₇O₅S

There total 15 articles about C₃₂H₄₅N₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₄N₂O₃

: 1421639-64-6
C₃₂H₄₅N₇O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid; water / dichloromethane / 0.5 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.5 h

With water; sodium hydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm3016987

Reference yield:

: 1394024-93-1
N₃-Phe-Leu-Leu-OMe

: 1421639-64-6
C₃₂H₄₅N₇O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / methanol / 15 h / 20 °C

2: tert.-butylnitrite; hydrogenchloride / 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide / 3 h / -30 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

4: trifluoroacetic acid / dichloromethane / 0.5 h

With hydrogenchloride; tert.-butylnitrite; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3016987

Reference yield:

: 2666-93-5
(S)-Leu-OMe

: 1421639-64-6
C₃₂H₄₅N₇O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V)

2: hydrazine hydrate / methanol / 15 h / 20 °C

3: tert.-butylnitrite; hydrogenchloride / 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide / 3 h / -30 °C

4: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

5: trifluoroacetic acid / dichloromethane / 0.5 h

With hydrogenchloride; tert.-butylnitrite; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3016987