1,3-di-tert-butyl-1,2,3,4-tetrahydro-6-isopropyl-2,4-bis(pentafluorophenyl)-1,3,5,2,4-triazadiborine

Base Information

• Chemical Name: 1,3-di-tert-butyl-1,2,3,4-tetrahydro-6-isopropyl-2,4-bis(pentafluorophenyl)-1,3,5,2,4-triazadiborine
• CAS No.: 172477-30-4
• Molecular Formula: C₂₄H₂₅B₂F₁₀N₃
• Molecular Weight: 567.089
• Mol file: 172477-30-4.mol

Synonyms:

Chemical Property of 1,3-di-tert-butyl-1,2,3,4-tetrahydro-6-isopropyl-2,4-bis(pentafluorophenyl)-1,3,5,2,4-triazadiborine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-di-tert-butyl-1,2,3,4-tetrahydro-6-isopropyl-2,4-bis(pentafluorophenyl)-1,3,5,2,4-triazadiborine

There total 2 articles about 1,3-di-tert-butyl-1,2,3,4-tetrahydro-6-isopropyl-2,4-bis(pentafluorophenyl)-1,3,5,2,4-triazadiborine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Isobutyronitrile (78-82-0) + (tert-butyl(trimethylsilyl)amino)chloro(pentafluorophenyl)borane (72886-50-1) → 1,3-di-tert-butyl-1,2,3,4-tetrahydro-6-isopropyl-2,4-bis(pentafluorophenyl)-1,3,5,2,4-triazadiborine (172477-30-4)

Guidance literature:

In dichloromethane; thermolysis of the substituted borane in the gas phase, condensing the product into a vessel containing 2-cyanopropane and CH2Cl2 cooled at -196°C, warming to -30°C, standing (overnight); filtration, crystn. (CH2Cl2); elem. anal.;

Reference yield:

bromopentafluorobenzene (344-04-7) → 1,3-di-tert-butyl-1,2,3,4-tetrahydro-6-isopropyl-2,4-bis(pentafluorophenyl)-1,3,5,2,4-triazadiborine (172477-30-4)

Guidance literature:

Multi-step reaction with 2 steps

1: BuLi / hexane; pentane

2: dichloromethane

With BuLi; In hexane; dichloromethane; pentane;

upstream raw materials:

Isobutyronitrile

(tert-butyl(trimethylsilyl)amino)chloro(pentafluorophenyl)borane

bromopentafluorobenzene