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C32H36N2O3

Base Information
  • Chemical Name:C32H36N2O3
  • CAS No.:312754-19-1
  • Molecular Formula:C32H36N2O3
  • Molecular Weight:496.649
  • Hs Code.:
C<sub>32</sub>H<sub>36</sub>N<sub>2</sub>O<sub>3</sub>

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Chemical Property of C32H36N2O3
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Technology Process of C32H36N2O3

There total 10 articles about C32H36N2O3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In butan-1-ol; at 100 ℃; for 1.25h; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.07.096
Guidance literature:
Multi-step reaction with 12 steps
1: potassium hexacyanoferrate(III); ammonia / water / 10 h / 80 °C / Inert atmosphere
2: tetrahydrofuran / 18 h / 25 °C
3: hydrogen; 10% Pd/C; sulfuric acid; acetic acid / 18 h / 25 °C / 760.05 Torr
4: sodium hydroxide / water / 1 h / 25 °C
5: triethylamine / dichloromethane / 1 h / 25 °C
6: aluminum (III) chloride / nitromethane / 4 h / 25 °C
7: hydrogen; 10% Pd/C / ethanol / 48 h / 25 °C / 760.05 Torr
8: aluminum (III) chloride / nitromethane / 3 h / 25 °C
9: hydrogen; 10% Pd/C / ethanol / 24 h / 25 °C / 760.05 Torr
10: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / Reflux
11: hydrogen; 10% Pd/C / ethanol / 18 h / 25 °C / 760.05 Torr
12: butan-1-ol / 1.25 h / 100 °C / Microwave irradiation
With aluminum (III) chloride; lithium aluminium tetrahydride; sulfuric acid; 10% Pd/C; ammonia; hydrogen; acetic acid; triethylamine; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; nitromethane; ethanol; dichloromethane; water; butan-1-ol; 6: |Friedel-Crafts Acylation / 8: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmcl.2012.07.096
Guidance literature:
Multi-step reaction with 6 steps
1: hydrogen; 10% Pd/C / ethanol / 48 h / 25 °C / 760.05 Torr
2: aluminum (III) chloride / nitromethane / 3 h / 25 °C
3: hydrogen; 10% Pd/C / ethanol / 24 h / 25 °C / 760.05 Torr
4: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / Reflux
5: hydrogen; 10% Pd/C / ethanol / 18 h / 25 °C / 760.05 Torr
6: butan-1-ol / 1.25 h / 100 °C / Microwave irradiation
With aluminum (III) chloride; lithium aluminium tetrahydride; 10% Pd/C; hydrogen; In tetrahydrofuran; nitromethane; ethanol; butan-1-ol; 2: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmcl.2012.07.096
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