Technology Process of C40H40N2O6
There total 3 articles about C40H40N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / dimethyl sulfoxide / 2.5 h / 40 °C / Inert atmosphere
2.1: iron(III) chloride / 1,2-dichloro-ethane / 1 h / 85 °C / Sealed tube
3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / chloroform / 0.5 h / 0 - 20 °C / Inert atmosphere
3.2: 1 h / 0 - 20 °C / Inert atmosphere
With
iron(III) chloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
chloroform; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201100049
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrahydrofuran / 1.5 h / -78 °C
2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / dimethyl sulfoxide / 2.5 h / 40 °C / Inert atmosphere
3.1: iron(III) chloride / 1,2-dichloro-ethane / 1 h / 85 °C / Sealed tube
4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / chloroform / 0.5 h / 0 - 20 °C / Inert atmosphere
4.2: 1 h / 0 - 20 °C / Inert atmosphere
With
iron(III) chloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
tetrahydrofuran; chloroform; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201100049
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: iron(III) chloride / 1,2-dichloro-ethane / 1 h / 85 °C / Sealed tube
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / chloroform / 0.5 h / 0 - 20 °C / Inert atmosphere
2.2: 1 h / 0 - 20 °C / Inert atmosphere
With
iron(III) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
chloroform; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201100049