Technology Process of 11-benzyloxy-4,9-dimethyl-6H-naphtho[2',3':4,5]furo[3,2-c]chromene-6,7,12-trione
There total 6 articles about 11-benzyloxy-4,9-dimethyl-6H-naphtho[2',3':4,5]furo[3,2-c]chromene-6,7,12-trione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) acetate monohydrate; potassium carbonate;
In
acetonitrile;
for 8h;
Inert atmosphere;
Reflux;
DOI:10.1039/c0ob01231a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Eaton's reagent / 5 h / 70 °C / Inert atmosphere
2: copper(II) acetate monohydrate; potassium carbonate / acetonitrile / 8 h / Inert atmosphere; Reflux
With
Eaton's reagent; copper(II) acetate monohydrate; potassium carbonate;
In
acetonitrile;
DOI:10.1039/c0ob01231a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzene / 0 - 20 °C / Inert atmosphere
2: silica gel / dichloromethane; benzene / 24 h / 20 °C / Inert atmosphere
3: silver(l) oxide / dichloromethane / 72 h / 20 °C / Inert atmosphere
4: copper(II) acetate monohydrate; potassium carbonate / acetonitrile / 8 h / Inert atmosphere; Reflux
With
copper(II) acetate monohydrate; silica gel; potassium carbonate; silver(l) oxide;
In
dichloromethane; acetonitrile; benzene;
1: Diels-Alder reaction;
DOI:10.1039/c0ob01231a
