Technology Process of C52H76N4O10
There total 5 articles about C52H76N4O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
2: Grubbs catalyst first generation / dichloromethane / Inert atmosphere; Reflux; Cooling with ice
With
Grubbs catalyst first generation; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
DOI:10.1021/ol201282d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium 10% on activated carbon; hydrogen / dichloromethane / 20 °C
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C
3: water; sodium hydroxide / tetrahydrofuran / 24 h / Reflux
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
5: Grubbs catalyst first generation / dichloromethane / Inert atmosphere; Reflux; Cooling with ice
With
Grubbs catalyst first generation; palladium 10% on activated carbon; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol201282d
- Guidance literature:
-
With
Grubbs catalyst first generation;
In
dichloromethane;
Inert atmosphere;
Reflux;
Cooling with ice;
DOI:10.1021/ol201282d
