Technology Process of C17H15N3O
There total 9 articles about C17H15N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere
2: pyridine; dmap / dichloromethane / 20 °C / Inert atmosphere
3: sodium azide / N,N-dimethyl-formamide / 60 °C / Inert atmosphere
4: copper(l) iodide / tetrahydrofuran / 50 °C / Inert atmosphere
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
6: hydrogenchloride; water / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere
7: dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere
With
pyridine; hydrogenchloride; dmap; copper(l) iodide; lithium aluminium tetrahydride; sodium azide; tetrabutyl ammonium fluoride; water;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
7: Swern oxidation;
DOI:10.1016/j.bmcl.2011.10.039
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide / tetrahydrofuran / 50 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
3: hydrogenchloride; water / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere
4: dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere
With
hydrogenchloride; copper(l) iodide; tetrabutyl ammonium fluoride; water;
In
tetrahydrofuran; dichloromethane;
4: Swern oxidation;
DOI:10.1016/j.bmcl.2011.10.039
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine; dmap / dichloromethane / 20 °C / Inert atmosphere
2: sodium azide / N,N-dimethyl-formamide / 60 °C / Inert atmosphere
3: copper(l) iodide / tetrahydrofuran / 50 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
5: hydrogenchloride; water / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere
6: dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere
With
pyridine; hydrogenchloride; dmap; copper(l) iodide; sodium azide; tetrabutyl ammonium fluoride; water;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
6: Swern oxidation;
DOI:10.1016/j.bmcl.2011.10.039